Manuel d'utilisation / d'entretien du produit 5975 du fabricant Agilent Technologies
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Agilent T echnologies 5975 Series Mass Selective Detectors Site Preparation Guide 5975 Series Site Prep.book Page 1 Thursday, January 31, 2008 9:47 AM.
Site Prepar ation Guide Notices © Agilent T e chnologies, Inc. 2008 No part of this manual ma y be reproduc ed in any form or by any means (including elec- tronic storage and retrieval or translation into a foreign language) without prior agree- ment and written consent from Agilent T echno logies, Inc.
Site Preparation Guide 3 Conten ts 1 General Inf ormati on Instrument I dentificati on 6 5975 MSD vers ions 6 Important Safety Warnings 7 Many inte rnal part s of the M SD carry d angerous voltages 7 .
4 Site Prepar ation Guide V oltage ran ges of ma jor comp onents 23 Power co nfig urat ions 24 Power re quiremen ts 25 Power pl ugs and cor d 2 6 Other electri cal consid eratio ns 27 Air Condi tio ni.
5 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s 1 Genera l Infor mati on Instrume nt Id entifi cation 6 Import ant Safety W arnings 7 Hydrog en Sa fety 9 Chemical .
6 Site Prepar ation Guide General In formation Instrument Identification Each 5975 Series Mass Selectiv e Detector ( MSD) is identified by a unique 10-character serial number . This serial number is located on a label on the low er lef t side nea r th e front of the instr u ment.
General Informati on Site Preparation Guide 7 Important Safety W arni ngs Bef ore mo ving on , there are sev eral im port ant saf ety noti ces that y ou should alwa y s k eep in mind when using the 5975 Series M ass S elective D etector .
8 Site Prepar ation Guide General In formation The use of incorrect or makeshift fuses or the shor t-circuiting of fuse holders creat es a shock ha zard f or t he operator an d can damage t he inst ru ment. Replac e fuse s only wit h fuse s of iden tical cu r rent rati ng and type.
General Informati on Site Preparation Guide 9 Hydrogen Safety Hydrogen gas may be used as car rier gas , and/or as fuel for cer t ain G C detec tors. When mixed wit h air , hydrogen can form ex plosive mixt ures. A detaile d discussion of h y drogen safety appears in Chapt er 1 of the Agile nt 5975 MSD Troubleshooting and Maintenance Manual.
10 Site Prepar ation Guide General In formation Chemical Safety W A RNING The foreline pump exhaust and split vent exhaust will con tain traces of the chemicals you are analyzing. These could potentially be toxic. V ent the foreline pump exhaust and spl it vent exhaust outside your labora tory or into a fume hood.
General Informati on Site Preparation Guide 11 Safety and Regulatory Cer tifications The 5975 Series M SD conf o rms to the follo wing saf ety standards: • Canadian Standards Associ a tion (CSA): C AN/CSA–C22.
12 Site Prepar ation Guide General In formation Symbols W arn ings in the man ual or on the instrument mu st be obse rve d during a ll phase s o f ope rat ion, ser vice , an d rep air of th is inst r umen t. F ailu re t o c omply with thes e precau tions violat es s afety st and ards of de sign and t he i nte nded use of the in str umen t.
General Informati on Site Preparation Guide 13 Electromagnetic compatibility This device complies with t he requiremen ts of CISPR 11. Operat ion is subject to the f ollo wing tw o cond itions: • This de vice ma y not caus e harmful interfer ence.
14 Site Prepar ation Guide General In formation Cleaning T o clean the unit, dis connect the po wer and wipe do wn wit h a dam p, lint- free cloth. Recycling the Produc t F or recyclin g, cont act y our local Agilen t sales office. 5975 Series Site Prep.
15 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s 2 Site Preparation Overview 16 Space and W eight Requireme nts 20 Communi cation s Requireme nts 22 Electr ical Re.
16 Site Prepar ation Guide Site Preparation Overview Bef ore the 5975 Series MSD system can be installed, the sit e must be properly prepa red. Site preparat ion include s, but is not li mited to, ensur ing that adequat e facili ties are available. Among th e site requ irement s are: • A dequat e space is available for t he MSD system .
Site Preparation Site Preparation Guide 17 • Com plying with all local la ws (co des, ord inances, and regu lation s) f or mechan ical, build ing, and elec trical distr ibuti on systems, hazar dous was t e disposa l, an d chemi cal s tora ge. Compliance must exist prior to installation.
18 Site Prepar ation Guide Site Preparation Ag ilent Technolo gies is not re sponsi ble for: • Any task n ot list ed in t he 5975 Series MSD T roubleshooting and Main te nanc e Man ual or the inst a.
Site Preparation Site Preparation Guide 19 Other documentat ion Additiona l infor matio n is co nt ained in t he following docum ent at ion: • 5975 Series MSD T roubleshooting and Maintenance Manual • 5975 Series MS D Operation man ual • 6890 Series GC manuals • GC acce ssories (autosam pler , etc.
20 Site Prepar ation Guide Site Preparation Space and W eight Requi rements Table 2 l ists dim ensi on an d weight infor mat ion for t h e MS D and rel ate d component s. Y our sit e must have enough benc h space for the MSD , GC, dat a system, a nd accessor ies (Figur e 1).
Site Preparation Site Preparation Guide 21 Ta b l e 2 Product dimens ions Approxima te Dimension s, cm (in) Produc t Heigh t Width Dept h W eight , kg ( lb) 5975 Seri e s MSD • G3170A D iffusion EI .
22 Site Prepar ation Guide Site Preparation Communication s Require ments Te l e p h o n e A tel ephone with a cord long enough t o be used at t he computer wil l allow the MSD ope r ator to commun icate with Agilen t Tech nologi es support personne l.
Site Preparation Site Preparation Guide 23 Electrical Requirements Y ou are res ponsible f or pro vidin g appr opriate elec trical po we r and po wer outlets f or all of the components in y our 5975 Series MSD system.
24 Site Prepar ation Guide Site Preparation Power configurations Electrical po wer for th e MSD must be single-phas e. The neutral wire cannot be used for safety grounding. The g round wire should car r y zero current ex cept for ground-fau lt cu rren t or st a tic elec tric d ischarge.
Site Preparation Site Preparation Guide 25 Power requirements Table 4 lists the po we r requirements f or t he 5975 Series MSD a n d related equipme nt. Extra po wer cap acity for future additio n s is rec ommended. Each pro duct listed r equir es a d edicated c ircuit.
26 Site Prepar ation Guide Site Preparation Power plugs and cord The MSD is supplied with a po w er cord and plug appropri ate f or the country from which t he order ori ginates.
Site Preparation Site Preparation Guide 27 Other electr ical considerat ions Additional electrica l consi deratio ns in clude: • Elec troma gnetic interfe renc e (EMI), such as is genera ted by NM Rs, radi o transmit ters, an d microwa ve link s, may inter fere with system perform ance.
28 Site Prepar ation Guide Site Preparation Air Conditioning and Envir onmental Requi rements Air co ndit ionin g cons idera tions inclu de t emperat ure, hu midi ty , air bor ne dust , and exhau st venting. Eac h of thes e is consid ered in more det ai l in the fol low i n g m a t e r i a l .
Site Preparation Site Preparation Guide 29 Airborne dust Agilent T echnolog ies recommends a ma ximum ai rborne particle dens ity of 55 μ g/m 3 . If y ou suspect y our site ex ceeds this l imit, co nt act y our local Agilen t T e chnologi es Cust omer Se rvice Organ ization.
30 Site Prepar ation Guide Site Preparation See your GC manu als for inform atio n on venting t he spli t vent. Fume (exhaust) hood An auxili ar y work space and fume hood are ne eded for some maint enance procedures.
Site Preparation Site Preparation Guide 31 Carrier and Reag ent Gas Requirements Table 6 list s the spec if ication s for the carr ier and reag ent gases. Pressur es and f l o ws a re as m easur ed at the bulkhe ad f itt ings on t he bac k of t he instr umen t, not at t he g as suppl y.
32 Site Prepar ation Guide Site Preparation Regulators, tubing, and fittings Y ou must supply appropriat e regulators for you r car rier and reagen t gas. • Regula tors m ust be dual-s ta ge. • Regul ators must hav e stainless -steel ( not e lastomer ic) diaphr agms.
Site Preparation Site Preparation Guide 33 Laboratory Suppl y Requirements Laborator y supply requirements vary wit h applicati ons. Cleaning solvents Cleaning t ask s for the M SD require t he follow.
34 Site Prepar ation Guide Site Preparation Spare parts a nd consumables The supplies and par ts list ed in Table 7 are used in the operati on and maintenance of a 5975 Series MSD sy stem. K eeping these parts on hand can reduc e sys tem do wntime r elate d to ins tr ument ma intenance an d repair .
Site Preparation Site Preparation Guide 35 Chemical Consu mables PF TBA (EI calib ration fluid) 05971-6 0571 PFDTD (CI calib ration fluid ) 8500-8130 EV AL A (eva luation sa mple) 05990-60045 OFN (Octafluor onapthalene) 5188-5348 OFN 100 fg/µL 5188-5347 Benzop h enone 85 00-5440 PFHT 5188-53 57 Foreline pump oil, P3, 0.
36 Site Prepar ation Guide Site Preparation 0.5-mm id , 85% V espel 15% graphite, for 0.32-mm id colum ns 5062-3506 0.8-mm id , 85% V espel 15% graphite, for 0.53-mm id colum ns 5062-3538 GC in let 0.27-mm id, 90% V espel 10 % graph ite, for 0. 10-mm id colum ns 5062-3518 0.
Site Preparation Site Preparation Guide 37 Receiving t he System When you r MSD sys tem is d elivere d, it is your resp onsi bilit y t o provide for remo val of the ship ping containers fr om the truck and thei r storage until inst al lation.
38 Site Prepar ation Guide Site Preparation Storage It is your respo nsibi lity to store the c ont ainer s unti l inst al lation . If your site does no t hav e adequat e st orage spac e, the c ont ainers may be stored at your expense i n a b onded wa rehouse.
Site Preparation Site Preparation Guide 39 Installation and V erification Installation Once the in stallatio n has beg un, it sho uld pro gress in a time ly manner to completion. D elays due t o inad equat e site preparation could c ause loss of instr ument use d uring t he warrant y period.
40 Site Prepar ation Guide Site Preparation Sensitivity specifications See the appro priate sensit ivity specifications f or your inst rument type. See the Agile nt T echnolo gies W eb site at http://www .agilent .com/ch em. NOTE SIM performance verification is not perf ormed at inst allation and must be purchased if desir ed.
41 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s A Power Cords This appendix sho ws t he pow er cords availabl e for the 5975 Series MSD. See page 26 for inf or mation a bout ensuring that the correct po wer cord is s upplied wit h your syst em .
42 Site Prepar ation Guide Power Cords Denm ark/Gr eenla nd, IEC 309 (Pa rt num ber 8120 -399 7) Austr alia/New Ze aland, AS 31 12-198 1 (Part numbe r 8120-136 9) India/S outh Africa , BS 546 (Par t numb er 8120 -4211) Israe l, SI 32 (Par t number 8120-5 182) Japan, NEMA L6-20 P (Part number G2025-601 89) 5975 Series Site Prep.
5975 Series Site Prep.book Page 43 Thursday, January 31, 2008 9:47 AM.
Agilent T echnologie s © Agilent T echnologies, Inc . Printed in USA, J a nuary 2008 5975 Series Site Prep.book Page 44 Thursday, January 31, 2008 9:47 AM.
Un point important après l'achat de l'appareil (ou même avant l'achat) est de lire le manuel d'utilisation. Nous devons le faire pour quelques raisons simples:
Si vous n'avez pas encore acheté Agilent Technologies 5975 c'est un bon moment pour vous familiariser avec les données de base sur le produit. Consulter d'abord les pages initiales du manuel d'utilisation, que vous trouverez ci-dessus. Vous devriez y trouver les données techniques les plus importants du Agilent Technologies 5975 - de cette manière, vous pouvez vérifier si l'équipement répond à vos besoins. Explorant les pages suivantes du manuel d'utilisation Agilent Technologies 5975, vous apprendrez toutes les caractéristiques du produit et des informations sur son fonctionnement. Les informations sur le Agilent Technologies 5975 va certainement vous aider à prendre une décision concernant l'achat.
Dans une situation où vous avez déjà le Agilent Technologies 5975, mais vous avez pas encore lu le manuel d'utilisation, vous devez le faire pour les raisons décrites ci-dessus,. Vous saurez alors si vous avez correctement utilisé les fonctions disponibles, et si vous avez commis des erreurs qui peuvent réduire la durée de vie du Agilent Technologies 5975.
Cependant, l'un des rôles les plus importants pour l'utilisateur joués par les manuels d'utilisateur est d'aider à résoudre les problèmes concernant le Agilent Technologies 5975. Presque toujours, vous y trouverez Troubleshooting, soit les pannes et les défaillances les plus fréquentes de l'apparei Agilent Technologies 5975 ainsi que les instructions sur la façon de les résoudre. Même si vous ne parvenez pas à résoudre le problème, le manuel d‘utilisation va vous montrer le chemin d'une nouvelle procédure – le contact avec le centre de service à la clientèle ou le service le plus proche.
